Nano-crystalline CoFe2O4 particles were synthesized through thermal decomposition of cobalt tartrate- ferric tartrate at 250, 450, 750 and 1050oC. The samples were characterized by XRD, DSC-TG, SEM, TEM and FT-IR. The XRD analysis showed that the sample calcined at 1050 oC exhibit pure spinel phase. The crystallite sizes lie in the range of 30 – 61 nm. The samples obtained at different calcination temperatures have different morphologies. The kinetics of thermal decomposition of metal tartrate mixtures were studied using non-isothermal thermogravimetric techniques. The thermal decomposition proceeds in three steps for cobalt iron (III) tartrate. The kinetic analysis of non-isothermal data of the decomposition reaction is best described by the Random nucleation in (three-dimentions) (A4) models. The activation parameters were calculated and the results of the dynamic integral methods were compared and discussed
Sameeh, M., Khairy, M., Bayoumy, W. A., El-asawi, T., & El-bellihi, A. (2014). Thermal Decomposition of Metal Tartrates through the Prepration of Nano Cobalt Ferrite. Journal of Basic and Environmental Sciences, 1(2), 46-64. doi: 10.21608/jbes.2014.369572
MLA
M. Sameeh; M. Khairy; W. A. Bayoumy; Tomader El-asawi; A.A. El-bellihi. "Thermal Decomposition of Metal Tartrates through the Prepration of Nano Cobalt Ferrite", Journal of Basic and Environmental Sciences, 1, 2, 2014, 46-64. doi: 10.21608/jbes.2014.369572
HARVARD
Sameeh, M., Khairy, M., Bayoumy, W. A., El-asawi, T., El-bellihi, A. (2014). 'Thermal Decomposition of Metal Tartrates through the Prepration of Nano Cobalt Ferrite', Journal of Basic and Environmental Sciences, 1(2), pp. 46-64. doi: 10.21608/jbes.2014.369572
VANCOUVER
Sameeh, M., Khairy, M., Bayoumy, W. A., El-asawi, T., El-bellihi, A. Thermal Decomposition of Metal Tartrates through the Prepration of Nano Cobalt Ferrite. Journal of Basic and Environmental Sciences, 2014; 1(2): 46-64. doi: 10.21608/jbes.2014.369572
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